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      • (Nano)Indentation models (conical indenters)
      • Correction factors and Correction of experimental data
      • Bilayer models to extract Young’s modulus of a thin film on a substrate (with conical indenters)
      • Multilayer models to extract Young’s moduli of thin films on a multilayer sample (with conical indenters)
      • Bilayer models to extract hardness of a thin film on a substrate (with conical indenters)
      • Multilayer models to extract hardness of thin films on a multilayer sample (with conical indenters)
      • Finite Element Modelling of conical indentation of thin film(s) on a substrate
    • Softwares
    • Reviews / Overviews of nanoindentation technique
    • Reviews / Overviews of nanoindentation technique applied to coatings
    • Books
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Links and References¶

Links¶

  • Guidata on Matlab website.
  • Matlab GUI.
  • Coding GUI behavior.
  • Visit the YAML website for more informations.
  • Visit the YAML code for Matlab.

Links about (nano)indentation¶

  • SF2M - Groupe Indentation.
  • Matlab Li’s code to determine elastic modulus and hardness of an ultra-thin film on a substrate using nanoindentation.
  • ISO 14577 - 1 , “Metallic materials – Instrumented indentation test for hardness and materials parameters – Part 1: Test method”, (2002).
  • ISO 14577 - 2 , “Metallic materials – Instrumented indentation test for hardness and materials parameters – Part 2: Verification and calibration of testing machines”, (2002).
  • ISO 14577 - 3 , “Metallic materials – Instrumented indentation test for hardness and materials parameters – Part 3: Calibration of reference blocks”, (2002).
  • ISO 14577 - 4 , “Metallic materials – Instrumented indentation test for hardness and materials parameters – Part 4: Test method for metallic and non-metallic coatings”, (2007).

References¶

  • Mercier D. et al., “Young’s modulus measurement of a thin film from experimental nanoindentation performed on multilayer systems” (2010).
  • Mercier D., “Behaviour laws of materials used in electrical contacts for « flip chip » technologies.”, PhD thesis (2013)
  • Mercier D., “Behaviour laws of materials used in electrical contacts for « flip chip » technologies.” PhD defense (2013).

(Nano)Indentation models (conical indenters)¶

  • Love A.E.H., “Boussinesq’s problem for a rigid cone.” (1939).
  • Galin L.A., “Spatial contact problems of the theory of elasticity for punches of circular shape in planar projection.”, J. Appl. Math. Mech. (PMM) (1946), 10, pp. 425-448.
  • Bulychev S.I. et al., “Determining Young’s modulus from the indentor penetration diagram.”, Zavod. Lab., 1973, 39, pp. 1137-1142.
  • Shorshorov M.K. et al., Sov. Phys. Dokl., 1982, 26.
  • Loubet J.L. et al., “Vickers Indentation Curves of Magnesium Oxide (MgO).” (1984).
  • Doerner M.F. and Nix W.D., “A method for interpreting the data from depth-sensing indentation instruments” (1986).
  • Loubet J.L. et al., “Vickers indentation curves of elastoplastic materials” (1986).
  • Joslin D.L. and Oliver W.C., “A new method for analyzing data from continuous depth-sensing microindentation tests” (1990).
  • Oliver W.C. and Pharr G.M., “An improved technique for determining hardness and elastic modulus using load and displacement sensing indentation experiments” (1992).
  • Pharr G.M. et al., “On the generality of the relationship among contact stiffness, contact area, and elastic modulus during indentation” (1992).
  • Loubet J.L. et al., “Nanoindentation with a surface force apparatus.” (1993).
  • Lucas B.N. et al., “Time Dependent Deformation During Indentation Testing.” (1996).
  • Hainsworth S.V. et al., “Analysis of nanoindentation load-displacement loading curves” (1996).
  • Bec S. et al., “Improvements in the indentation method with a surface force apparatus” (1996).
  • Menčík J. et al., “Determination of elastic modulus of thin layers using nanoindentation” (1997).
  • Bolshakov A. and Pharr G. M., “Influences of pile-up on the measurement of mechanical properties by load and depth sensing indentation techniques.” (1998).
  • Cheng Y.T. and Cheng C.M. ,”Effects of ‘sinking in’ and ‘piling up’ on estimating the contact area under load in indentation.” (1998).
  • Cheng Y.T. and Cheng C.M. ,”Relationships between hardness, elastic modulus, and the work of indentation.” (1998).
  • Hochstetter G. et al., “Strain-rate effects on hardness of glassy polymers in the nanoscale range. Comparison between quasi-static and continuous stiffness measurements” (1999).
  • Malzbender J. and de With G., “Indentation load–displacement curve, plastic deformation, and energy.” (2002).
  • Li X. and Bhushan B., “A review of nanoindentation continuous stiffness measurement technique and its applications.” (2002).
  • Oliver W.C. and Pharr G.M., “Measurement of hardness and elastic modulus by instrumented indentation: Advances in understanding and refinements to methodology” (2004).
  • Cheng Y.T. and Cheng C.M., “Scaling, dimensional analysis, and indentation measurements.” (2004).
  • Fischer-Cripps A.C., “Critical review of analysis and interpretation of nanoindentation test data” (2006).
  • Guillonneau G. et al.,”Extraction of mechanical properties with second harmonic detection for dynamic nanoindentation testing.” (2012).
  • Guillonneau G. et al., “Determination of mechanical properties by nanoindentation independently of indentation depth measurement” (2012).
  • Yetna N’jock M. et al., “A criterion to identify sinking-in and piling-up in indentation of materials.” (2015).

Correction factors and Correction of experimental data¶

  • King R.B., “Elastic analysis of some punch problems for a layered medium” (1987).
  • Menčík J., “Determination of elastic modulus of thin layers using nanoindentation” (1997).
  • Hay J.C. et al., “A critical examination of the fundamental relations used in the analysis of nanoindentation data” (1999).
  • Troyon M. and Lafaye S., “About the importance of introducing a correction factor in the Sneddon relationship for nanoindentation measurements” (2002).
  • Strader J.H. et al., “An experimental evaluation of the constant b relating the contact stiffness to the contact area in nanoindentation.” (2006).
  • Fischer-Cripps A.C., “Critical review of analysis and interpretation of nanoindentation test data” (2006).
  • Jakes J.E. et al., “Experimental method to account for structural compliance in nanoindentation measurements” (2008).
  • Pharr G.M. et al., “Critical issues in making small-depth mechanical property measurements by nanoindentation with continuous stiffness measurement” (2009).
  • Kaufman J. D. and Klapperich C. M., “Surface detection errors cause overestimation of the modulus in nanoindentation on soft materials” (2009).
  • Li H. et al., “New methods of analyzing indentation experiments on very thin films” (2010).
  • Piccarolo S. et al., “Improving surface detection on nanoindentation of compliant materials” (2010).

Bilayer models to extract Young’s modulus of a thin film on a substrate (with conical indenters)¶

  • Bückle H., “VDI Berichte” (1961).
  • Doerner M.F. and Nix W.D.,”A method for interpreting the data from depth-sensing indentation instruments” (1986).
  • Yu H.Y. et al., “The effect of substrate on the elastic properties of films determined by the indentation test - axisymmetric Boussinesq problem” (1990).
  • Pharr G.M. and Oliver W.C., “Measurement of Thin Film Mechanical Properties Using Nanoindentation” (1992).
  • Gao H. et al., “Elastic contact versus indentation modeling of multi-layered materials” (1992).
  • Menčík J. et al., “Determination of elastic modulus of thin layers using nanoindentation” (1997).
  • Chen X. and Vlassak J.J., “Numerical study on the measurement of thin film mechanical properties by means of nanoindentation” (2001).
  • Rar A. et al., “Assessment of new relation for the elastic compliance of a film–substrate system.” (2002).
  • Saha R. and Nix W.D., “Effects of the substrate on the determination of thin film mechanical properties by nanoindentation” (2002).
  • Chen S. et al., “Nanoindentation of thin-film-substrate system: Determination of film hardness and Young’s modulus” (2004).
  • Jung Y.-G. et al. “Evaluation of elastic modulus and hardness of thin films by nanoindentation” (2004).
  • Perriot A. and Barthel E., “Elastic contact to a coated half-space: Effective elastic modulus and real penetration” (2004).
  • Bec S. et al., “A simple guide to determine elastic properties of films on substrate from nanoindentation experiments” (2006).
  • Xu H. and Pharr G.M., “An improved relation for the effective elastic compliance of a film/substrate system during indentation by a flat cylindrical punch.” (2006).
  • Korsunsky A.M. and Constantinescu A., “The influence of indenter bluntness on the apparent contact stiffness of thin coatings” (2009).
  • Li H. and Vlassak J.J., “Determining the elastic modulus and hardness of an ultra-thin film on a substrate using nanoindentation” (2009).
  • Sakai M., “Substrate-affected indentation contact parameters of elastoplastic coating/substrate composites” (2009).
  • Hay J. and Crawford B., “Measuring substrate-independent modulus of thin films” (2011).
  • Bull S.J., “Mechanical response of atomic layer deposition alumina coatings on stiff and compliant substrates” (2011).
  • Bull S.J., “A simple method for the assessment of the contact modulus for coated systems.” (2014).
  • Li Y. et al., “Models for nanoindentation of compliant films on stiff substrates” (2015).

Multilayer models to extract Young’s moduli of thin films on a multilayer sample (with conical indenters)¶

  • Pailler-Mattei C. et al., “In vivo measurements of the elastic mechanical properties of human skin by indentation tests” (2008).
  • Mercier D. et al., “Young’s modulus measurement of a thin film from experimental nanoindentation performed on multilayer systems” (2010).
  • Mercier D., “Lois de comportement des matériaux utilisés dans les contacts électriques pour application ” flip chip “” (2013).
  • Constantinescu A. et al., “Symbolic and numerical solution of the axisymmetric indentation problem for a multilayered elastic coating” (2013).
  • Puchi-Cabrera. E.S. et al., “A description of the composite elastic modulus of multilayer coated systems” (2015).

Bilayer models to extract hardness of a thin film on a substrate (with conical indenters)¶

  • Bückle H., “VDI Berichte” (1961).
  • Kao P.-W. and Byrne J. G., “Ion Implantation Effects on Fatigue and Surface Hardness” (1981).
  • Jönsson B. and Hogmark S., “Hardness measurements of thin films” (1984).
  • Doerner M.F. et al., “Plastic properties of thin films on substrates as measured by submicron indentation hardness and substrate curvature techniques” (1986).
  • Burnett P.J. and Rickerby D.S., “The mechanical properties of wear-resistant coatings: I: Modelling of hardness behaviour.” (1987).
  • Burnett P.J. and Rickerby D.S., “The mechanical properties of wear-resistant coatings: II: Experimental studies and interpretation of hardness.” (1987).
  • Page T.F. et al., “Nanoindentation Characterisation of Coated Systems: P:S2 - A New Approach Using the Continuous Stiffness Technique” (1998).
  • Fernandes J.V. et al., “A model for coated surface hardness” (2000).
  • Han S.M. et al., “Combinatorial studies of mechanical properties of Ti–Al thin films using nanoindentation” (2005).
  • Han S.M. et al., “Determining hardness of thin films in elastically mismatched film-on-substrate systems using nanoindentation” (2006).

Multilayer models to extract hardness of thin films on a multilayer sample (with conical indenters)¶

  • Engel P.A. et al., “Interpretation of superficial hardness for multilayer platings*” (1992).
  • Rahmoun K. et al., “A multilayer model for describing hardness variations of aged porous silicon low-dielectric-constant thin films” (2009).
  • Arrazat B. et al., “Nano indentation de couches dures ultra minces de ruthénium sur or” (2010).

Finite Element Modelling of conical indentation of thin film(s) on a substrate¶

  • Charleux L., “Abapy Documentation”
  • ABAQUS documentation
  • Bhattacharya A.K. and Nix W.D., “Finite element analysis of cone indentation.” (1991).
  • Madsen D.T. et al. “Finite Element Simulation of Indentation Behavior of thin Films.” (1991).
  • Sun Y. et al., “Finite element analysis of the critical ratio of coating thickness to indentation depth for coating property measurements by nanoindentation.” (1995).
  • Hubert N. et al. “Identification of elastic-plastic material parameters from pyramidal indentation of thin films.” (2002).
  • He J.L. and Veprek S., “Finite element modeling of indentation into superhard coatings.” (2003).
  • Cai X. and Bangert H., “Hardness measurements of thin films-determining the critical ratio of depth to thickness using FEM.” (2005).
  • Bolshakov A. and Pharr G.M., “Influences of pile-up on the measurement of mechanical properties by load and depth sensing indentation techniques.” (1998)
  • Lichinchi M. et al., “Simulation of Berkovich nanoindentation experiments on thin films using finite element method.” (1998).
  • Chen X. and Vlassak J.J., “A Finite Element Study on the Nanoindentation of Thin Films.” (2000).
  • Chen X. and Vlassak J.J., “Numerical study on the measurement of thin film mechanical properties by means of nanoindentation.” (2001).
  • Bouzakis K.-D. et al., “Thin hard coatings stress–strain curve determination through a FEM supported evaluation of nanoindentation test results.”, (2001).
  • Xu Z.-H. and Rowcliffe D., “Finite element analysis of substrate effects on indentation behaviour of thin films.” (2004).
  • Panich N. and Sun Y. “Effect of penetration depth on indentation response of soft coatings on hard substrates: a finite element analysis” (2004)
  • Bressan J.D. et al., “Modeling of nanoindentation of bulk and thin film by finite element method.” (2005).
  • Pelletier H. et al., “Characterization of mechanical properties of thin films using nanoindentation test.” (2006)
  • Xu H., “A Finite Element Study of the Contact Stiffness of Homogenous Materials and Thin Films.” PhD thesis - University of Tennessee - Knoxville (2007)
  • Antunes J.M. et al., “On the determination of the Young’s modulus of thin films using indentation tests” (2007).
  • Chen S.H. et al., “Small scale, grain size and substrate effects in nano-indentation experiment of film–substrate systems.” (2007).
  • Huang X. and Pelegri A.A., “Finite element analysis on nanoindentation with friction contact at the film/substrate interface.” (2007).
  • Pelegri A.A. and Huang X., “Nanoindentation on soft film/hard substrate and hard film/soft substrate material systems with finite element analysis.” (2008).
  • Wittler O. et al., “Mechanical characterisation of thin metal layers by modelling of the nanoindentation experiment.” (2008).
  • Sakharova N.A. et al., “Comparison between Berkovich, Vickers and conical indentation tests: A three-dimensional numerical simulation study.” (2009).
  • Chen C., “2-D Finite Element Modeling for Nanoindentation and Fracture Stress Analysis.” PhD thesis - University of South Florida (2009).
  • Moore S.W. et al., “Nanoindentation in elastoplastic materials: insights from numerical simulations.” (2010).
  • Dowhan L. et al., “Investigation of thin films by nanoindentation with doe and numerical methods.” (2011).
  • Isselé H. et al., “Determination of the Young’s modulus of a TiN Thin Film by nanoindentation: analytical models and numerical FEM simulation.” (2012).
  • Phiciato’s blog (2013)
  • Moćko W. et al., “Simulation of nanoindentation experiments of single-layer and double-layer thin films using finite element method.” (2014).
  • Kibech S. et al., “Nanoindentation” (2014).
  • Kopernik M. and Milenin A., “Numerical modeling of substrate effect on determination of elastic and plastic properties of TiN nanocoating in nanoindentation test.” (2014).
  • Li Y. et al., “Models for nanoindentation of compliant films on stiff substrates” (2015).
  • Gupta A. K. et al., “Evaluation of elasto-plastic properties of ITO film using combined nanoindentation and finite element approach” (2015).

Softwares¶

  • IndentAnalyser by ASMEC
  • Elastica by ASMEC
  • Softwares from SIOMEC
  • Softwares from Keysight
  • Piuma dataviewer
  • Punias
  • Gwyddion
  • Softwares from Nanovea
  • Virtual nanoindenter
  • Nanoindentation from Kibech S. et al.

Reviews / Overviews of nanoindentation technique¶

  • Li X. and Bhushan B., “A review of nanoindentation continuous stiffness measurement technique and its applications.” (2002).
  • VanLandingham M.R., “Review of Instrumented Indentation” (2003).
  • Fischer-Cripps A.C., “Nanoindentation” Springer 3rd Ed. (2011).
  • Oliver W.C. and Pharr G.M., “Measurement of hardness and elastic modulus by instrumented indentation: Advances in understanding and refinements to methodology” (2004).
  • Fischer-Cripps A.C., “Critical review of analysis and interpretation of nanoindentation test data” (2006).
  • Lucca D.A. et al., “Nanoindentation: Measuring methods and applications” (2012).
  • Němeček J., “Nanoindentation in Material Science” (2012).
  • Michailidis N. et al., “Nanoindentation” (2014).

Reviews / Overviews of nanoindentation technique applied to coatings¶

  • Pharr G.M. and Oliver W.C., “Measurement of Thin Film Mechanical Properties Using Nanoindentation” (1992).
  • Mencík J. et al., “Determination of elastic modulus of thin layers using nanoindentation” (1997).
  • Nix W.D., “Elastic and plastic properties of thin films on substrates: nanoindentation techniques” (1997).
  • Van Vliet K.J. and Gouldstone A., “Mechanical Properties of Thin Films Quantified Via Instrumented Indentation” (2001).
  • Fischer-Cripps A.C., “Nanoindentation” Springer 3rd Ed. (2011).
  • Šimůnková Š., “Mechanical properties of thin film–substrate systems” (2003).
  • Bull S.J., “Nanoindentation of coatings” (2005).

Books¶

  • Johnson K.L., “Contact Mechanics” (1987), ISBN - 9780521347969.
  • Bhushan B., “Micro/Nanotribology and Its Applications” (1997).
  • Fischer-Cripps A.C., “Introduction to Contact Mechanics” Springer 1st Ed. (2000).
  • Fischer-Cripps A.C., “Nanoindentation” Springer 1st Ed. (2002).
  • Fischer-Cripps A.C., “Nanoindentation” Springer 2nd Ed. (2004).
  • Fischer-Cripps A.C., “Introduction to Contact Mechanics” Springer 2nd Ed. (2007).
  • Fischer-Cripps A.C., “Nanoindentation” Springer 3rd Ed. (2011).
  • Tiwari A., “Nanomechanical Analysis of High Performance Materials” Springer Vol. 203 (2014).
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